TA Instruments

AR1718-0001f

04/09/2012 17:57:53

Sample name	ASW 10 mm from base, 60 mm to top, disk 21 Provil novo medium texture
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1718
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 17:57:53

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-5.179	7.928	-0.6533	1.0280	22.4	1371	5.6268	10000	0.3364	21.81	7.0336	703.36	3.384E-3	0.0	1.0	61.028	-15.889	6.342
0.7930	12.36	0.06415	2.0160	22.4	1358	13.3608	10000	0.3334	8.888	16.701	1670.1	3.384E-3	0.0	1.0	62.016	2.4328	9.889
1.605	19.37	0.08286	3.0200	22.4	1370	27.0328	10000	0.3362	3.653	33.791	3379.1	3.384E-3	0.1	1.1	63.020	4.9226	15.49
2.216	23.04	0.09618	4.0200	22.4	1375	40.8605	10000	0.3374	2.590	51.076	5107.6	3.384E-3	0.1	1.1	64.020	6.7982	18.43
3.596	30.85	0.1166	5.0160	22.4	1380	67.6150	10000	0.3386	1.450	84.519	8451.9	3.384E-3	0.1	1.1	65.016	11.033	24.68
5.579	39.49	0.1413	5.9960	22.4	1362	106.7060	10000	0.3344	0.8737	133.38	13338	3.384E-3	0.1	1.1	65.996	17.117	31.59
6.255	42.54	0.1470	7.0160	22.4	1357	126.3480	10000	0.3331	0.7501	157.94	15794	3.384E-3	0.1	1.1	67.016	19.189	34.03
7.799	49.13	0.1587	7.9920	22.4	1361	165.3140	10000	0.3342	0.5640	206.64	20664	3.384E-3	0.1	1.1	67.992	23.926	39.31
9.976	57.54	0.1734	9.0160	22.4	1371	223.3950	10000	0.3366	0.4142	279.24	27924	3.384E-3	0.2	1.2	69.016	30.606	46.03
12.34	63.69	0.1937	10.024	22.4	1361	274.8200	10000	0.3340	0.3354	343.53	34353	3.383E-3	0.2	1.2	70.024	37.846	50.95
14.18	69.65	0.2036	11.016	22.4	1365	326.0350	10000	0.3350	0.2814	407.54	40754	3.384E-3	0.2	1.2	71.016	43.506	55.72
16.11	75.11	0.2144	12.004	22.4	1356	377.1490	10000	0.3327	0.2403	471.44	47144	3.383E-3	0.2	1.2	72.004	49.413	60.09
18.05	80.51	0.2243	13.028	22.4	1350	434.6650	10000	0.3313	0.2083	543.33	54333	3.384E-3	0.2	1.2	73.028	55.390	64.41
20.37	86.43	0.2357	13.992	22.4	1340	498.5440	10000	0.3289	0.1794	623.18	62318	3.384E-3	0.2	1.2	73.992	62.505	69.14
23.74	94.60	0.2510	15.016	22.4	1354	595.1320	10000	0.3323	0.1513	743.92	74392	3.384E-3	0.3	1.3	75.016	72.845	75.68
25.97	99.91	0.2599	16.016	22.4	1348	664.5000	10000	0.3309	0.1351	830.63	83063	3.384E-3	0.3	1.3	76.016	79.673	79.93
28.40	105.7	0.2688	16.996	22.4	1351	740.5720	10000	0.3315	0.1210	925.72	92572	3.383E-3	0.3	1.3	76.996	87.130	84.52
31.96	113.7	0.2810	18.020	22.4	1342	855.0170	10000	0.3293	0.1037	1068.8	1.0688E5	3.383E-3	0.3	1.3	78.020	98.047	90.98
34.24	118.8	0.2883	19.016	22.4	1345	931.1280	10000	0.3301	0.09531	1163.9	1.1639E5	3.384E-3	0.3	1.3	79.016	105.05	95.03
36.86	124.2	0.2967	20.032	22.4	1337	1020.0800	10000	0.3281	0.08659	1275.1	1.2751E5	3.383E-3	0.3	1.3	80.032	113.10	99.40
40.61	132.3	0.3070	20.992	22.4	1334	1153.2700	10000	0.3275	0.07625	1441.6	1.4416E5	3.383E-3	0.3	1.3	80.992	124.60	105.8
43.59	137.4	0.3173	22.016	22.4	1321	1242.0601	10000	0.3242	0.07000	1552.6	1.5526E5	3.384E-3	0.4	1.4	82.016	133.72	109.9
46.47	142.8	0.3254	23.016	22.4	1311	1343.5699	10000	0.3218	0.06430	1679.5	1.6795E5	3.384E-3	0.4	1.4	83.016	142.56	114.2
50.72	150.8	0.3363	23.992	22.4	1324	1495.5800	10000	0.3250	0.05823	1869.5	1.8695E5	3.384E-3	0.4	1.4	83.992	155.61	120.6
53.38	155.9	0.3424	25.016	22.4	1311	1597.0000	10000	0.3218	0.05393	1996.3	1.9963E5	3.383E-3	0.4	1.4	85.016	163.77	124.7
56.77	161.3	0.3519	26.016	22.4	1304	1711.0200	10000	0.3200	0.05009	2138.8	2.1388E5	3.384E-3	0.4	1.4	86.016	174.15	129.1
61.92	169.3	0.3657	27.016	22.4	1299	1881.9399	10000	0.3187	0.04530	2352.4	2.3524E5	3.383E-3	0.5	1.5	87.016	189.97	135.5
64.85	174.4	0.3717	27.992	22.4	1299	1999.1400	10000	0.3189	0.04271	2498.9	2.4989E5	3.384E-3	0.5	1.5	87.992	198.95	139.6
67.69	179.6	0.3770	29.016	22.4	1293	2116.0300	10000	0.3173	0.04010	2645.0	2.6450E5	3.384E-3	0.5	1.5	89.016	207.66	143.6
72.36	187.5	0.3858	30.016	22.4	1290	2305.8201	10000	0.3165	0.03666	2882.3	2.8823E5	3.383E-3	0.5	1.5	90.016	221.99	150.0
76.03	192.7	0.3946	31.016	22.4	1272	2433.0701	10000	0.3122	0.03426	3041.3	3.0413E5	3.383E-3	0.5	1.5	91.016	233.27	154.2
79.84	197.8	0.4036	31.992	22.4	1261	2637.6101	10000	0.3094	0.03221	3297.0	3.2970E5	3.383E-3	0.5	1.5	91.992	244.93	158.3
85.24	205.8	0.4142	32.988	22.4	1272	2774.0200	10000	0.3122	0.03003	3467.5	3.4675E5	3.383E-3	0.5	1.5	92.988	261.52	164.7
88.59	211.0	0.4199	34.016	22.4	1271	2913.7900	10000	0.3120	0.02856	3642.2	3.6422E5	3.383E-3	0.6	1.6	94.016	271.78	168.8
94.82	218.6	0.4338	35.016	22.4	1253	3127.3999	10000	0.3076	0.02623	3909.3	3.9093E5	3.383E-3	0.6	1.6	95.016	290.92	174.9
98.44	223.9	0.4396	36.016	22.4	1244	3279.1599	10000	0.3054	0.02482	4099.0	4.0990E5	3.384E-3	0.6	1.6	96.016	301.99	179.1
101.3	229.1	0.4423	36.996	22.4	1242	3430.6599	10000	0.3047	0.02366	4288.3	4.2883E5	3.384E-3	0.6	1.6	96.996	310.88	183.3
107.0	236.6	0.4520	38.016	22.4	1233	3658.0500	10000	0.3025	0.02201	4572.6	4.5726E5	3.383E-3	0.6	1.6	98.016	328.16	189.3
110.9	241.8	0.4585	39.016	22.4	1233	3822.3401	10000	0.3027	0.02109	4777.9	4.7779E5	3.384E-3	0.7	1.7	99.016	340.18	193.5
116.8	249.6	0.4679	40.016	22.4	1220	4068.3999	10000	0.2995	0.01959	5085.5	5.0855E5	3.383E-3	0.7	1.7	100.016	358.26	199.7
120.3	254.6	0.4725	40.996	22.4	1217	4233.0698	10000	0.2987	0.01877	5291.3	5.2913E5	3.383E-3	0.7	1.7	100.996	369.11	203.7
125.9	262.5	0.4797	42.016	22.4	1190	4499.1602	10000	0.2922	0.01728	5624.0	5.6240E5	3.383E-3	0.7	1.7	102.016	386.27	210.0
131.4	267.6	0.4910	42.992	22.4	1183	4676.0000	10000	0.2903	0.01652	5845.0	5.8450E5	3.383E-3	0.7	1.7	102.992	403.13	214.1
136.8	272.7	0.5015	43.992	22.4	1199	4851.3301	10000	0.2944	0.01613	6064.2	6.0642E5	3.383E-3	0.7	1.7	103.992	419.56	218.1
144.0	280.3	0.5138	44.996	22.4	1171	5129.0298	10000	0.2873	0.01489	6411.3	6.4113E5	3.383E-3	0.7	1.7	104.996	441.90	224.3
147.0	285.5	0.5149	45.992	22.4	1183	5318.2002	10000	0.2903	0.01451	6647.8	6.6478E5	3.384E-3	0.8	1.8	105.992	451.01	228.4
154.0	293.1	0.5254	47.024	22.4	1177	5602.0698	10000	0.2889	0.01370	7002.6	7.0026E5	3.384E-3	0.8	1.8	107.024	472.44	234.5
158.1	298.1	0.5302	48.016	22.4	1163	5797.6299	10000	0.2855	0.01308	7247.0	7.2470E5	3.384E-3	0.8	1.8	108.016	484.94	238.5
162.9	303.3	0.5372	49.024	22.4	1151	6102.2500	10000	0.2824	0.01251	7627.8	7.6278E5	3.384E-3	0.8	1.8	109.024	499.91	242.7
172.2	311.0	0.5536	49.992	22.4	1140	6302.2700	10000	0.2798	0.01179	7877.8	7.8778E5	3.384E-3	0.8	1.8	109.992	528.17	248.8
175.2	316.0	0.5543	51.016	22.4	1141	6510.3501	10000	0.2800	0.01142	8137.9	8.1379E5	3.384E-3	0.9	1.9	111.016	537.36	252.8
181.9	323.8	0.5619	52.016	22.4	1135	6832.2100	10000	0.2786	0.01083	8540.3	8.5403E5	3.383E-3	0.9	1.9	112.016	558.17	259.0
187.4	328.9	0.5700	52.996	22.4	1109	7046.3999	10000	0.2721	0.01025	8808.0	8.8080E5	3.384E-3	0.9	1.9	112.996	575.05	263.1
193.4	336.4	0.5748	54.016	22.4	1080	7374.3799	10000	0.2652	9.546E-3	9218.0	9.2180E5	3.384E-3	0.9	1.9	114.016	593.31	269.1
197.5	341.6	0.5781	55.016	22.4	1094	7601.3501	10000	0.2684	9.372E-3	9501.7	9.5017E5	3.384E-3	0.9	1.9	115.016	605.86	273.3
204.0	346.7	0.5883	55.988	22.4	1107	7828.4702	10000	0.2717	9.209E-3	9785.6	9.7856E5	3.384E-3	0.9	1.9	115.988	625.77	277.4
211.4	354.2	0.5967	57.028	22.4	1085	8168.9600	10000	0.2662	8.644E-3	10211	1.0211E6	3.384E-3	1.0	2.0	117.028	648.43	283.4
218.1	359.3	0.6070	58.016	22.4	1085	8408.3604	10000	0.2664	8.406E-3	10510	1.0510E6	3.383E-3	1.0	2.0	118.016	669.17	287.5
225.0	367.0	0.6131	58.992	22.4	1069	8769.2500	10000	0.2623	7.936E-3	10962	1.0962E6	3.383E-3	1.0	2.0	118.992	690.32	293.6
230.2	372.0	0.6189	59.992	22.4	1030	9008.3701	10000	0.2528	7.443E-3	11260	1.1260E6	3.383E-3	1.0	2.0	119.992	706.35	297.6

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

231.6	375.0	0.6175	1.0040	22.4	1055	301.7330	10000	0.2589	7.501E-3	377.17	37717	3.383E-3	0.0	2.0	122.004	710.40	300.0
232.7	375.0	0.6205	2.0040	22.4	1005	553.2530	10000	0.2467	7.148E-3	691.57	69157	3.384E-3	0.0	2.1	123.004	713.85	300.0
234.2	375.0	0.6245	3.0200	22.4	1028	807.9320	10000	0.2522	7.307E-3	1009.9	1.0099E5	3.383E-3	0.1	2.1	124.020	718.45	300.0
235.4	375.0	0.6278	4.0040	22.4	1031	1181.6300	10000	0.2530	7.330E-3	1477.0	1.4770E5	3.383E-3	0.1	2.1	125.004	722.31	300.0
233.0	375.0	0.6214	5.0200	22.4	1123	1432.9500	10000	0.2755	7.984E-3	1791.2	1.7912E5	3.383E-3	0.1	2.1	126.020	714.88	300.0
234.6	375.0	0.6256	6.0240	22.4	1039	1810.9900	10000	0.2550	7.389E-3	2263.7	2.2637E5	3.384E-3	0.1	2.1	127.024	719.82	300.0
233.7	375.0	0.6233	7.0200	22.4	1045	2061.0801	10000	0.2565	7.431E-3	2576.4	2.5764E5	3.384E-3	0.1	2.1	128.020	717.03	300.0
230.6	375.0	0.6149	8.0040	22.4	1103	2312.3401	10000	0.2707	7.841E-3	2890.4	2.8904E5	3.384E-3	0.1	2.2	129.004	707.49	300.0
233.6	375.0	0.6229	9.0200	22.4	1048	2689.4199	10000	0.2573	7.454E-3	3361.8	3.3618E5	3.384E-3	0.2	2.2	130.020	716.69	300.0
233.6	375.0	0.6229	10.008	22.4	1009	2940.8201	10000	0.2477	7.178E-3	3676.0	3.6760E5	3.384E-3	0.2	2.2	131.008	716.64	300.0
232.0	375.0	0.6188	11.004	22.4	1028	3319.3301	10000	0.2522	7.307E-3	4149.2	4.1492E5	3.383E-3	0.2	2.2	132.004	711.89	300.0
229.4	375.0	0.6117	12.020	22.4	1018	3569.0901	10000	0.2498	7.237E-3	4461.4	4.4614E5	3.383E-3	0.2	2.2	133.020	703.72	300.0
233.2	375.0	0.6217	13.000	22.4	1069	3820.4500	10000	0.2623	7.601E-3	4775.6	4.7756E5	3.383E-3	0.2	2.2	134.000	715.31	300.0
232.5	375.0	0.6199	14.028	22.4	1040	4197.4399	10000	0.2552	7.395E-3	5246.8	5.2468E5	3.384E-3	0.2	2.3	135.028	713.21	300.0
233.4	375.0	0.6224	15.004	22.4	1066	4448.8501	10000	0.2617	7.583E-3	5561.1	5.5611E5	3.384E-3	0.3	2.3	136.004	716.03	300.0
233.4	375.0	0.6223	16.008	22.4	1076	4829.9902	10000	0.2642	7.654E-3	6037.5	6.0375E5	3.383E-3	0.3	2.3	137.008	715.94	300.0
232.3	375.0	0.6196	17.020	22.4	1056	5079.3398	10000	0.2593	7.513E-3	6349.2	6.3492E5	3.383E-3	0.3	2.3	138.020	712.80	300.0
230.0	375.0	0.6133	18.004	22.4	1094	5328.5801	10000	0.2684	7.777E-3	6660.7	6.6607E5	3.383E-3	0.3	2.3	139.004	705.55	300.0
233.9	375.0	0.6236	19.008	22.4	1051	5705.3799	10000	0.2579	7.471E-3	7131.7	7.1317E5	3.383E-3	0.3	2.3	140.008	717.52	300.0
230.5	375.0	0.6146	20.020	22.4	1069	5956.7998	10000	0.2623	7.601E-3	7446.0	7.4460E5	3.384E-3	0.3	2.4	141.020	707.13	300.0
228.4	375.0	0.6092	21.004	22.4	1052	6207.9800	10000	0.2581	7.477E-3	7760.0	7.7600E5	3.384E-3	0.4	2.4	142.004	700.86	300.0
234.4	375.0	0.6251	22.004	22.4	1032	6585.2598	10000	0.2532	7.336E-3	8231.6	8.2316E5	3.384E-3	0.4	2.4	143.004	719.24	300.0
230.9	375.0	0.6158	23.000	22.4	1043	6836.3701	10000	0.2560	7.419E-3	8545.5	8.5455E5	3.384E-3	0.4	2.4	144.000	708.45	300.0
231.8	375.0	0.6182	24.008	22.4	1055	7213.4702	10000	0.2589	7.501E-3	9016.8	9.0168E5	3.384E-3	0.4	2.4	145.008	711.27	300.0
232.2	375.0	0.6192	25.024	22.4	1014	7464.5898	10000	0.2489	7.213E-3	9330.7	9.3307E5	3.384E-3	0.4	2.4	146.024	712.38	300.0
231.3	375.0	0.6169	26.020	22.4	1013	7716.0898	10000	0.2487	7.207E-3	9645.1	9.6451E5	3.384E-3	0.4	2.5	147.020	709.74	300.0
233.7	375.0	0.6231	27.004	22.4	1043	8096.5200	10000	0.2560	7.418E-3	10121	1.0121E6	3.384E-3	0.5	2.5	148.004	716.88	300.0
233.6	375.0	0.6230	28.000	22.4	1068	8344.4697	10000	0.2621	7.595E-3	10431	1.0431E6	3.383E-3	0.5	2.5	149.000	716.78	300.0
234.3	375.0	0.6248	29.020	22.4	1059	8723.6904	10000	0.2599	7.530E-3	10905	1.0905E6	3.384E-3	0.5	2.5	150.020	718.83	300.0
231.7	375.0	0.6179	30.004	22.4	1064	8972.7197	10000	0.2611	7.565E-3	11216	1.1216E6	3.384E-3	0.5	2.5	151.004	710.88	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

234.1	372.2	0.6290	1.0040	22.4	1028	224.8910	10000	0.2524	7.422E-3	281.11	28111	3.384E-3	0.0	2.5	152.004	718.28	297.8
224.3	364.7	0.6150	2.0040	22.4	1059	581.7980	10000	0.2599	7.963E-3	727.25	72725	3.384E-3	0.0	2.6	153.004	688.02	291.7
218.0	359.6	0.6062	3.0400	22.4	1075	821.5310	10000	0.2640	8.318E-3	1026.9	1.0269E5	3.384E-3	0.1	2.6	154.040	668.71	287.7
209.4	351.9	0.5950	4.0200	22.4	1082	1172.1700	10000	0.2656	8.739E-3	1465.2	1.4652E5	3.384E-3	0.1	2.6	155.020	642.35	281.5
204.2	346.9	0.5885	5.0040	22.4	1111	1395.8900	10000	0.2727	9.232E-3	1744.9	1.7449E5	3.384E-3	0.1	2.6	156.004	626.38	277.5
195.4	339.3	0.5760	6.0160	22.4	1073	1734.0000	10000	0.2634	9.322E-3	2167.5	2.1675E5	3.383E-3	0.1	2.6	157.016	599.56	271.4
192.2	334.1	0.5752	7.0160	22.4	1101	1959.4000	10000	0.2703	9.865E-3	2449.3	2.4493E5	3.384E-3	0.1	2.6	158.016	589.61	267.3
186.8	329.0	0.5676	8.0000	22.4	1104	2172.2900	10000	0.2711	0.01020	2715.4	2.7154E5	3.384E-3	0.1	2.7	159.000	573.04	263.2
179.5	321.4	0.5584	8.9960	22.4	1105	2493.4900	10000	0.2713	0.01070	3116.9	3.1169E5	3.384E-3	0.1	2.7	159.996	550.68	257.2
175.5	316.3	0.5548	10.020	22.4	1118	2704.4399	10000	0.2745	0.01118	3380.6	3.3806E5	3.384E-3	0.2	2.7	161.020	538.41	253.0
167.1	308.6	0.5414	11.000	22.4	1152	3011.1299	10000	0.2828	0.01210	3763.9	3.7639E5	3.383E-3	0.2	2.7	162.000	512.59	246.9
164.0	303.6	0.5403	12.000	22.4	1163	3211.4099	10000	0.2855	0.01262	4014.3	4.0143E5	3.383E-3	0.2	2.7	163.000	503.24	242.9
157.8	295.8	0.5334	13.004	22.4	1155	3513.0701	10000	0.2834	0.01320	4391.3	4.3913E5	3.384E-3	0.2	2.7	164.004	484.12	236.7
154.0	290.8	0.5295	14.000	22.4	1151	3699.4800	10000	0.2824	0.01361	4624.4	4.6244E5	3.384E-3	0.2	2.8	165.000	472.41	232.6
147.0	285.8	0.5146	15.016	22.4	1191	3887.1101	10000	0.2924	0.01459	4858.9	4.8589E5	3.384E-3	0.3	2.8	166.016	451.10	228.6
140.6	278.0	0.5059	16.004	22.4	1174	4168.7500	10000	0.2881	0.01519	5210.9	5.2109E5	3.383E-3	0.3	2.8	167.004	431.49	222.4
136.5	272.8	0.5003	17.020	22.4	1195	4350.1099	10000	0.2934	0.01606	5437.6	5.4376E5	3.383E-3	0.3	2.8	168.020	418.81	218.3
130.6	265.3	0.4922	18.000	22.4	1203	4612.6699	10000	0.2952	0.01709	5765.8	5.7658E5	3.383E-3	0.3	2.8	169.000	400.56	212.2
125.6	260.1	0.4828	19.004	22.4	1204	4788.4902	10000	0.2956	0.01780	5985.6	5.9856E5	3.384E-3	0.3	2.8	170.004	385.33	208.1
122.7	254.9	0.4815	20.000	22.4	1205	4962.9102	10000	0.2958	0.01856	6203.6	6.2036E5	3.384E-3	0.3	2.9	171.000	376.50	203.9
115.3	247.3	0.4662	21.004	22.4	1223	5206.7900	10000	0.3003	0.02001	6508.5	6.5085E5	3.383E-3	0.4	2.9	172.004	353.68	197.8
111.0	242.1	0.4585	22.016	22.4	1227	5369.2798	10000	0.3011	0.02093	6711.6	6.7116E5	3.384E-3	0.4	2.9	173.016	340.55	193.7
106.1	234.3	0.4530	23.000	22.4	1237	5606.9702	10000	0.3035	0.02253	7008.7	7.0087E5	3.384E-3	0.4	2.9	174.000	325.63	187.4
102.9	229.3	0.4487	24.004	22.4	1242	5757.9102	10000	0.3049	0.02363	7197.4	7.1974E5	3.383E-3	0.4	2.9	175.004	315.64	183.4
96.42	221.6	0.4352	25.024	22.4	1256	5982.7202	10000	0.3082	0.02558	7478.4	7.4784E5	3.383E-3	0.4	2.9	176.024	295.83	177.3
91.99	216.3	0.4253	26.000	22.4	1265	6132.7300	10000	0.3104	0.02704	7665.9	7.6659E5	3.383E-3	0.4	3.0	177.000	282.21	173.0
88.55	211.2	0.4193	27.076	22.4	1268	6339.3301	10000	0.3112	0.02843	7924.2	7.9242E5	3.384E-3	0.5	3.0	178.076	271.66	168.9
82.28	203.5	0.4043	28.004	22.4	1250	6475.4600	10000	0.3068	0.03018	8094.3	8.0943E5	3.384E-3	0.5	3.0	179.004	252.42	162.8
79.71	198.2	0.4022	29.000	22.4	1285	6612.7900	10000	0.3153	0.03270	8266.0	8.2660E5	3.384E-3	0.5	3.0	180.000	244.54	158.6
75.98	192.9	0.3939	30.020	22.4	1283	6808.4600	10000	0.3149	0.03448	8510.6	8.5106E5	3.384E-3	0.5	3.0	181.020	233.11	154.3
71.64	185.2	0.3868	31.000	22.4	1287	6932.1401	10000	0.3159	0.03752	8665.2	8.6652E5	3.384E-3	0.5	3.0	182.000	219.79	148.2
68.76	179.9	0.3821	32.000	22.4	1271	7057.5400	10000	0.3118	0.03925	8821.9	8.8219E5	3.383E-3	0.5	3.1	183.000	210.94	143.9
62.94	172.1	0.3657	33.000	22.4	1303	7232.4302	10000	0.3198	0.04398	9040.5	9.0405E5	3.383E-3	0.6	3.1	184.000	193.10	137.7
59.03	167.0	0.3535	34.016	22.4	1294	7343.1099	10000	0.3175	0.04639	9178.9	9.1789E5	3.384E-3	0.6	3.1	185.016	181.09	133.6
56.43	161.7	0.3490	35.000	22.4	1304	7457.1499	10000	0.3202	0.04989	9321.4	9.3214E5	3.383E-3	0.6	3.1	186.000	173.13	129.4
51.32	153.6	0.3341	36.004	22.4	1294	7618.1299	10000	0.3175	0.05483	9522.7	9.5227E5	3.383E-3	0.6	3.1	187.004	157.46	122.9
49.79	148.5	0.3353	37.000	22.4	1313	7717.1499	10000	0.3222	0.05954	9646.4	9.6464E5	3.384E-3	0.6	3.1	188.000	152.77	118.8
46.16	143.2	0.3223	38.000	22.4	1319	7817.0098	10000	0.3238	0.06433	9771.3	9.7713E5	3.384E-3	0.6	3.2	189.000	141.62	114.6
41.50	135.1	0.3072	39.004	22.4	1332	7960.0298	10000	0.3269	0.07299	9950.0	9.9500E5	3.383E-3	0.7	3.2	190.004	127.31	108.1
39.84	130.0	0.3065	40.016	22.4	1326	8047.1099	10000	0.3254	0.07848	10059	1.0059E6	3.384E-3	0.7	3.2	191.016	122.23	104.0
37.01	124.7	0.2968	41.016	22.4	1329	8134.8301	10000	0.3262	0.08549	10169	1.0169E6	3.384E-3	0.7	3.2	192.016	113.55	99.76
32.90	116.5	0.2823	42.016	22.4	1313	8258.5596	10000	0.3222	0.09669	10323	1.0323E6	3.383E-3	0.7	3.2	193.016	100.93	93.21
30.61	111.5	0.2747	43.016	22.4	1327	8333.1201	10000	0.3256	0.1068	10416	1.0416E6	3.383E-3	0.7	3.2	194.016	93.925	89.16
28.26	106.2	0.2662	44.000	22.4	1325	8407.6299	10000	0.3252	0.1176	10510	1.0510E6	3.384E-3	0.7	3.3	195.000	86.708	84.92
26.11	100.6	0.2596	45.000	22.4	1327	8482.4004	10000	0.3256	0.1312	10603	1.0603E6	3.384E-3	0.8	3.3	196.000	80.109	80.46
22.10	92.38	0.2392	46.000	22.4	1349	8581.2900	10000	0.3311	0.1581	10727	1.0727E6	3.384E-3	0.8	3.3	197.000	67.795	73.90
20.15	87.03	0.2315	47.008	22.4	1339	8643.2695	10000	0.3287	0.1768	10804	1.0804E6	3.384E-3	0.8	3.3	198.008	61.821	69.62
18.47	81.34	0.2271	48.000	22.4	1342	8705.0703	10000	0.3293	0.2028	10881	1.0881E6	3.384E-3	0.8	3.3	199.000	56.661	65.07
16.18	75.56	0.2141	49.000	22.4	1333	8760.9502	10000	0.3271	0.2334	10951	1.0951E6	3.384E-3	0.8	3.3	200.000	49.626	60.45
13.15	67.54	0.1947	50.000	22.4	1341	8834.8398	10000	0.3291	0.2939	11044	1.1044E6	3.384E-3	0.8	3.4	201.000	40.355	54.03
11.22	61.64	0.1820	51.000	22.4	1352	8883.8203	10000	0.3319	0.3559	11105	1.1105E6	3.384E-3	0.9	3.4	202.000	34.417	49.32
9.590	55.58	0.1726	52.008	22.4	1358	8926.7002	10000	0.3334	0.4397	11158	1.1158E6	3.383E-3	0.9	3.4	203.008	29.423	44.46
8.082	50.19	0.1610	53.020	22.4	1351	8963.4805	10000	0.3315	0.5362	11204	1.1204E6	3.383E-3	0.9	3.4	204.020	24.794	40.15
6.382	44.18	0.1444	54.016	22.4	1352	9000.0000	10000	0.3317	0.6924	11250	1.1250E6	3.383E-3	0.9	3.4	205.016	19.579	35.34
4.839	37.91	0.1276	55.016	22.4	1358	9030.2803	10000	0.3334	0.9451	11288	1.1288E6	3.383E-3	0.9	3.4	206.016	14.845	30.33
3.583	32.58	0.1100	56.000	22.4	1358	9054.5596	10000	0.3334	1.280	11318	1.1318E6	3.383E-3	0.9	3.5	207.000	10.992	26.06
2.618	26.26	0.09969	57.016	22.4	1366	9078.2803	10000	0.3354	1.982	11348	1.1348E6	3.383E-3	1.0	3.5	208.016	8.0314	21.01
2.060	22.52	0.09146	58.020	22.4	1367	9089.8496	10000	0.3356	2.696	11362	1.1362E6	3.383E-3	1.0	3.5	209.020	6.3187	18.02
1.010	14.22	0.07103	59.016	22.4	1354	9106.6797	10000	0.3323	6.695	11383	1.1383E6	3.384E-3	1.0	3.5	210.016	3.0991	11.38
0.3724	7.411	0.05025	60.000	22.4	1371	9114.6797	10000	0.3366	24.97	11393	1.1393E6	3.384E-3	1.0	3.5	211.000	1.1425	5.929

